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The development of innovative measuring technology for process optimization in hot rolling mills becomes more and more relevant because of increasing demands on product quality. Measurement technology for high-resolution non-contact cross-sectional area measurement has shown that the variation in cross-sectional area contains information about the rolling process. This information can be used for the development of new measurement devices and analytical methods for process optimization. The harsh environmental conditions and strict safety regulations result in great effort when implementing a new sensor prototype in hot rolling mills. For this reason, this work presents a mechatronic test stand that can simulate the cross-sectional area variation under laboratory conditions realistically.
A Large and Quick Induction Field Scanner for Examining the Interior of Extended Objects or Humans
(2017)
This study describes the techniques and signal properties of a large, powerful, and linear-scanning 1.5 MHz induction field scanner. The mechanical system is capable of quickly reading the volume of relative large objects, e.g., a test person. The general approach mirrors Magnetic Induction Tomography (MIT), but the details differ considerably from currently-described MIT systems: the setup is asymmetrical, and it operates in gradiometric modalities, either with coaxial excitation with destructive interference or with a single excitation loop and tilted receivers. Following this approach, the primary signals were almost completely nulled, and test objects' real or imaginary imprint was obtained directly. The coaxial gradiometer appeared advantageous: exposure to strong fields was reduced due to destructive interference. Meanwhile, the signals included enhanced components at higher spatial frequencies, thereby obtaining a gradually improved capability for localization. For robust signals, the excitation field can be powered towards the rated limits of human exposure to time-varying magnetic fields. Repeated measurements assessed the important signal integrity, which is affected by the scanner´s imperfections, particularly any motions or respiratory changes in living beings during or between repeated scans. The currently achieved and overall figure of merit for artifacts was 58 dB for inanimate test objects and 44 dB for a test person. Both numbers should be understood as worst case levels: a repeated scan with intermediate breathing and drift/dislocations requires 50 seconds, whereas a single measurement (with respiratory arrest) takes only about 5 seconds.
This experimental study demonstrates for the first time a solid-state circuitry and design for a simple compact copper coil (without an additional bulky permanent magnet or bulky electromagnet) as a contactless electromagnetic acoustic transducer (EMAT) for pulse echo operation at MHz frequencies. A pulsed ultrasound emission into a metallic test object is electromagnetically excited by
an intense MHz burst at up to 500 A through the 0.15 mm filaments of the transducer. Immediately thereafter, a smoother and quasi “DC-like” current of 100 A is applied for about 1 ms and allows an
echo detection. The ultrasonic pulse echo operation for a simple, compact, non-contacting copper coil is new. Application scenarios for compact transducer techniques include very narrow and
hostile environments, in which, e.g., quickly moving metal parts must be tested with only one, non-contacting ultrasound shot. The small transducer coil can be operated remotely with a cable
connection, separate from the much bulkier supply circuitry. Several options for more technical and fundamental progress are discussed.
Photoluminescence (PL) in GaN or InGaN layers monitored during epitaxial growth at high temperatures permits a quasi-continuous in situ characterization of opto-electronic properties. Therefore, epitaxial parameters can now be optimized at the earliest possible stage. A pulsed and high-power UV laser was required for PL excitation at high temperatures. Herein, the underlying nonlinear mechanism was studied via time-resolved PL experiments and rate equation-based modeling. A temperature-activated and saturable path for quenching over defects was identified. Beyond the saturation threshold, reasonably-intensive PL sets in. At high temperatures not only is the near band gap-PL present, but also—as a new observation—a defect-assisted PL emerges. Apart from these specific electronic transitions in high-temperature PL of GaN, a simple, but reasonably predictive model of the luminescent thin film has been set up to track down interference fringes in the PL spectra. It is worth mentioning that the spectral PL modulation (aiming at the Purcell effect) is often mixed up with ordinary Fabry–Pérot interference. A distinction has become key to properly analyze the spectral signatures of high-temperature PL in order to provide a reliable in situ characterization of GaN layers during epitaxial growth
Gallium Nitride (GaN) and Indium Gallium Nitride (InGaN) have become important semiconductor materials for the LED lighting industry. Recently, a photoluminescence (PL) technique for direct in-situ characterization of GaN and InGaN layers during epitaxial growth in a planetary metalorganic vapor phase epitaxy (MOVPE) reactor was reported. The PL signals reveal – at the earliest possible stage – information about current layer thickness, temperature, composition, surface roughness, and self-absorption. Thus, the PL data is valuable for both controlling and optimizing the growth parameters, thereby promising both better devices and a better yield for the LED industry. This technical report describes an extension of this PL technique to close coupled showerhead (CCS) reactors with narrow optical viewports. In contrast to the wide aperture optics in previous investigations, a compact and all-fiber optical probe without voluminous lens optics, filter elements or beam splitters was used.
A simple copper coil without a voluminous stationary magnet can be utilized as a non-contacting transmitter and as a detector for ultrasonic vibrations in metals. Advantages of such compact EMATs without (electro-)magnet might be: applications in critical environments (hot, narrow, presence of iron filings…), potentially superior fields (then improved ultrasound transmission and more sensitive ultrasound detection).
The induction field of an EMAT strongly influences ultrasound transduction in the nearby metal. Herein, a simplified analytical method for field description at high liftoff is presented. Within certain limitations this method reasonably describes magnetic fields (and resulting eddy currents, inductances, Lorentz forces, acoustic pressures) of even complex coil arrangements. The methods can be adapted to conventional EMATS with a separate stationary magnet.
Increased distances (liftoff) are challenging and technically relevant, and this practical question is addressed: with limited electrical power and given free space between transducer and target metal, what would be the most efficient geometry of a circular coil? Furthermore, more complex coil geometries (“butterfly coil”) with a concentrated field and relatively higher reach are briefly investigated.
In this work we report the first quasi-continuous in-situ photoluminescence study of growing InGaN LED structures inside an industrial-grade metal-organic vapor phase epitaxy (MOVPE) reactor at growth temperature. The photoluminescence spectra contain information about temperature, thickness and composition of the epitaxial layers. Furthermore, the in-situ spectra – even at an early stage of the growth of the active region – can be used to predict the photoluminescence emission wavelength of the structure at room temperature. In this study an accuracy of this predicted wavelength in the range of ± 1.3 nm (2σ) is demonstrated. This technique thus appears suitable for closed-loop control of the emission wavelength of InGaN LEDs already during growth.
Electro-magnetic acoustic transducers (EMATs) are intended as non-contact and non-destructive ultrasound transducers for metallic material. The transmitted intensities from EMATS are modest, particularly at notable lift off distances. Some time ago a concept for a “coil only EMAT” was presented, without static magnetic field. In this contribution, such compact “coil only EMATs” with effective areas of 1–5 cm2 were driven to excessive power levels at MHz frequencies, using pulsed power technologies. RF induction currents of 10 kA and tens of Megawatts are applied. With increasing power the electroacoustic conversion efficiency also increases. The total effect is of second order or quadratic, therefore non-linear and progressive, and yields strong ultrasound signals up to kW/cm2 at MHz frequencies in the metal. Even at considerable lift off distances (cm) the ultrasound can be readily detected. Test materials are aluminum, ferromagnetic steel and stainless steel (non-ferromagnetic). Thereby, most metal types are represented. The technique is compared experimentally with other non-contact methods: laser pulse induced ultrasound and spark induced ultrasound, both damaging to the test object’s surface. At small lift off distances, the intensity from this EMAT concept clearly outperforms the laser pulses or heavy spark impacts.
Efficient photoluminescence (PL) spectra from GaN and InGaN layers at temperatures up to 1100 K are observed with low noise floor and high dynamic resolution. A number of detailed spectral features in the PL can be directly linked to physical properties of the epitaxial grown layer. The method is suggested as an in situ monitoring tool during epitaxy of nitride LED and laser structures. Layer properties like thickness, band gap or film temperature distribution are feasible.
To analyze the electric field around bipolar resectoscopes, used in urology, in terms of reasons for late complications after a surgical treatment a flexible multielectrode system was developed to measure the 3-D potential distribution. A high spatial resolution is achieved with the least possible individual measurements under the conditions of a quasi-static electric field. A flexible arrangement and positioning of the measuring points in the vertical direction of the experimental environment enable an adjustable spatial resolution and the selection of the region of interest. The existing influence of the multielectrode system on the measuring results is described and a correction method is presented to achieve significant results. Thus, the multielectrode system is usable for a comparative study of bipolar resectoscopes varying in the arrangement of resection and return electrode.